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Molybdenum hexacarbonyl reacts with 2,4-dimethylpyridine, 3-butylpyridine or 4-methylquinoline in refluxing acetonitrile to give the respective ligand complexes [Mo(CO)4(2,4-Me2py)2], [Mo(CO)5(3-Bupy)] and [Mo(CO)5(4-methylquinoline)]. The complexes have been characterized by IR, PMR, mass spectra and elemental analysis.
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Reference：
Chiral nitrogen ligands in late transition metal-catalysed asymmetric synthesis—I. Addressing the problem of ligand lability in rhodium-catalysed hydrosilations,
Nitrogen-Containing Ligands for Asymmetric Homogeneous and Heterogeneous Catalysis