The effect of the change of 110-70-3 synthetic route on the product

This molecular description is the mechanism of the reaction; it describes how individual atoms, ions, or molecules interact to form particular products.If you are interested, you can also browse other articles of 110-70-3, We look forward to the emergence of more reaction modes in the future.

110-70-3, An elementary termolecular reaction involves the simultaneous collision of three atoms, molecules, or ions.33527-91-2, name is Tris[2-(dimethylamino)ethyl]amine. Here is a downstream synthesis route of the compound 33527-91-2

To a stirred solution of Lambda/,Lambda/’-dimethylethylene diamine (3.66 mL, 34 mmol) in dichloromethane (40 mL) at 0C was added dropwise a solution of di-tert-butyl dicarbonate (2.4 g, 11 mmol) in dichloromethane (20 mL) and allowed to warm to room temperature overnight, concentrated under reduced pressure, diluted with EtOAc (100 mL), washed with water (2 * 100 mL), brine (100 mL), dried and concentrated under reduced pressure to give the title product 91 as a colourless oil (1.54 g, 74% yield). 1H NMR (400 MHz, CDCI3) delta 3.26 (t, J = 6.15 Hz, 2H), 2.81 (s, 3H), 2.66 (t, J = 6.57 Hz, 2H), 2.38 (s, 3H), 9.28 (s, 9H) ppm.

This molecular description is the mechanism of the reaction; it describes how individual atoms, ions, or molecules interact to form particular products.If you are interested, you can also browse other articles of 110-70-3, We look forward to the emergence of more reaction modes in the future.

Reference£º
Patent; ANTIKOR BIOPHARMA LIMITED; DEONARAIN, Mahendra Persaud; YAHIOGLU, Gokhan; STAMATI, Ioanna; SAOUROS, Savvas; KAPADNIS, Prashant Bhimrao; (423 pag.)WO2016/46574; (2016); A1;,
Chiral nitrogen ligands in late transition metal-catalysed asymmetric synthesis¡ªI. Addressing the problem of ligand lability in rhodium-catalysed hydrosilations
Nitrogen-Containing Ligands for Asymmetric Homogeneous and Heterogeneous Catalysis