110-70-3, The molecularity of an elementary reaction is the number of molecules that collide during that step in the mechanism. If there is only a single reactant molecule in an elementary reaction, that step is designated as unimolecular. 110-70-3, name is N1,N2-Dimethylethane-1,2-diamine. A new synthetic method of this compound is introduced below.
EXAMPLE 12 N-Boc-N,N’-dimethylethylene diamine N,N’-dimethyl ethylenediamine (8.8 g) was dissolved in 200 ml tetrahydrofuran and to this was added over a 10 min period di-t-butyldicarbonate (4.36 g) in 30 mL tetrahydrofuran. 72 hours later, the solvent was evaporated and the residue partitioned between ether and KHCO3 and the organic layer was dried (MgSO4) and evaporated to give 11.6 g title compound (58% yield). 300 MHz 1 H NMR was consistent with proposed structure.
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Reference£º
Patent; G. D. Searle & Co.; US4902706; (1990); A;,
Chiral nitrogen ligands in late transition metal-catalysed asymmetric synthesis¡ªI. Addressing the problem of ligand lability in rhodium-catalysed hydrosilations
Nitrogen-Containing Ligands for Asymmetric Homogeneous and Heterogeneous Catalysis